Chemical analysis

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30 Terms

1

What is a pure substance

A pure substance is a single element/compound not mixed with any other substance

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2

What is a formulation?

A mixture that has been designed as a useful product

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3

What is chromatography used for?

To separate mixtures and help identify substances

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4

What is the equation for Rf value

Rf= distance moved by substance/distance moved by solvent

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5

How can we identify substances through chromatography?

Different compounds have differend Rf values so compounds with the same Rf values are the same

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6

What is the test for hydrogen?

ā€˜squeaky pop test'

ā†³ Burning splint creates a pop sound if hydrogen is present

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7

What is the test for oxygen?

Glowing splint

ā†³ splint relights if oxygen is present

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8

What is the test for carbon dioxide?

Lime water ā†’ turns cloudy if carbon dioxide is present

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9

What is the test for chlorine?

Damp litmus paper ā†’ bleached and turns white

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10

What colour flame does a lithium compound produce?

Crimson

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11

What colour flame does a sodium compounds produce?

Yellow

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12

What colour flame does a potassium compound produce?

Lilac

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13

What colour flame does a copper compound produce?

Green

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14

What colour flame does a calcium compound produce?

Orange-red

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15

What happens if sodum hydroxide is added to calcium and magnesium?

white precipitate is produced

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16

What happens when sodium hydroxide is added to aluminium?

Forms a white precipitate which dissolves when excess sodium hydroxide is added

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17

what happens when sodium hydroxide is added to copper(II)?

A blue precipitate is formed

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18

What happens when sodium hydroxide is added to Iron (II)?

A green precipitate is formed

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19

What happens when sodium hydroxide is added to Iron (III)

A brown precipitate is formed

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20

What is the test for carbonate (CO32-) ions?

Dilute acid ā†’ bubbles are given off

ā†³ test bubbles with limewater

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21

What is the test for sulfate ions?

  • Add a few drops of dilute hydrochloric acid

  • Add a few drops of barium chloride solution

    ā†³ a white precipitate is formed if sulfate ions are present

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22

Explain why, in a test for sulfate ions, the sample is acidified with hydrochloric acid first

  • Carbonate ions also produce a white precipitate with barium chloride solution

  • Acid reacts with any carbonate ions present and removes them

  • Which prevents a false negative

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23

What is the test for halide ions?

  • Add a few drops of nitric acid

  • Add a few drops of dilute silver nitrate solution

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24

What is formed when chloride ions react with silver nitrate?

A white precipitate

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25

What is formed when bromide ions react with silver nitrate?

A cream precipitate

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26

what is formed when iodide reacts with silver nitrate

A yellow precipitate

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27

What are the advantages of using instrumental methods of anlysis?

Gives improved:

  • Speed

  • Accuracy

  • Sensitivity

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28

Name 1 example of an instrumental method of analysis

  • Flame emission spectroscopy

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29

How are metal ions and their concentrations identified using flame emission spectroscopy?

  • The sample is put into a flame

  • The light given out is passed through a spectroscope

  • This produces a line spectrum that can me analysed

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30
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