Chemistry 3.3.6 Organic Analysis (copy)

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Ionisation, Acceleration, Drift, Detection.

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AQA A Level Chemistry Mass Spectrometry

10 Terms

1

Ionisation, Acceleration, Drift, Detection.

What are the 4 stages of Mass Spectrometry?

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2

1500-500 - It's unique to each compound, and can be compared against known fingerprint regions to spot differences.

What is the fingerprint region?

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3

1 peak

How many peaks for 1 type of bond on IR spec

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4

Add NaOH and warm, then acidify the HNO3 and add AgNO3, a ppt will form due to the formation of Ag + the halogen

Cl= white

Br= Cream

I= Yellow

How do you test for haloalkanes?

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5

Add acidified potassium dichromate and heat

colour change from orange to green for 1/2 alcohols no change for 3

How do you test for alcohols

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6

Warm feelings, blue → brick red ppt

OR

Warm tollens → silver mirror formation (Ag)

2 ways to test for aldehydes

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7

Add sodium carbonate → CO2 released (effervesences)

How do you test for carboxylic acids?

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8

Constantly vibrating and can absorb IR in the same frequency

Why do chemical bonds absorb IR

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9

faster vibrations

What effect does a stronger bond have on the frequency of vibrations

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10

Beam of IR with a range of frequencies passed through samples

radiation that emerges is missing frequencies that have nit be absorbed by the bond

What happens inside a IR spectrometer

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