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What is an acid
An acid is a species that is a proton donor
What is a base
A base is a proton acceptor
Amphoteric
When a substance has both acidic and basic components, such as an amino acid
Preparing a standard solution
Accurately weigh out mass of solid using weighing boat and scale and record.
Transfer solid to a 250cm3 beaker, rinse weighing boat with distilled water to ensure all solid is transferred
Transfer solution to a 250cm3 flask using a funnel. Rinse funnel and beaker with distilled water to ensure all solution has been transferred.
Add 50-100cm3 of distilled water and swirl around to mix. Then add distilled water until below calibration mark.
Then using a dropping pipette add distilled water until meniscus sits on the mark.
Place stopper on flask and invert at least 10 times to fully mix.
Carrying out titration
Rinse burette with solution that will fill it, HCl, then fill burette with solution. Ensur3e burette tip is full with no air bubbles.
Record initial burette reading to 0.05cm2
Rinse a pipette with the solution you will transfer to the conical flask (CacO3). Use a pipette + safety filler to transfer 25.0 cm³ of the other solution into a 250 cm³ conical flask (the acid).
Add 2-3 drops of suitable indicator. Phenolphthalein for weak acid vs strong base. Methyl orange for strong acid vs weak base.
Place a white tile under the conical flask to see the colour change more clearly.
Run the burette solution slowly into the flask while swirling. As you approach the end point, add the solution dropwise.
Stop when the first permanent colour change is observed:
Phenolphthalein: pink → colourless or colourless → pale pink
Methyl orange: yellow → orange/red or vice versa
Record the final burette reading to 2 d.p.
Calculate the titre (final − initial).
Repeat until concordant results obtained (0.10cm3 of each other. Find mean.
Strong acid vs weak acid
A strong acid fully dissociate in water whilst a weak acid partially dissociates in water. Most weak acids are organic