Recrystallisation of a sample of benzoic acid

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Key steps and observations in the procedure to recrystallise a sample of benzoic acid:

  • a known mass of benzoic acid crystals are dissolved in a minimum amount of hot water

  • the solution is filtered use a heated funnel to remove insoluble impurities

  • the solution in cooled in ice, and a seed crystal is added to speed up the process

  • the crystals are collected by vaccuum filtration which separates benzoic acid from soluble impurities

  • crystals air dry and their mass is obtained

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Why is the minimum amount of hot water used

  • benzoic acid is very soluble in hot water

  • the more solvent the less crystals will be obtained

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