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LAB 2 — Acidification of Sodium Benzoate
Reactant(s):
Sodium benzoate (C₆H₅COO⁻ Na⁺)
Hydrochloric acid (HCl)
Water (solvent)
Product(s):
Benzoic acid (solid) ← MAIN PRODUCT
NaCl (aqueous)
LAB 3 — Acid–Base Extraction
Reactant(s) (the mixture you start with):
Benzoic acid
2-naphthol
Naphthalene
Diethyl ether (organic solvent)
Reagents added:
Sodium bicarbonate (NaHCO₃)
Sodium hydroxide (NaOH)
Hydrochloric acid (HCl)
Product(s):
You end with three separate purified solids:
Benzoic acid (re-acidified from NaHCO₃ extract)
2-naphthol (re-acidified from NaOH extract)
Naphthalene (already neutral, isolated from organic layer)
LAB 5 — Distillation of Unknown Liquid
Reactant(s):
A liquid mixture (two miscible organic liquids)
Product(s):
Lower-boiling liquid distillate (the purified component)
Higher-boiling component stays in flask
You also identify the product using density + boiling point.
LAB 8 — Hydrolysis of Methyl Salicylate → Salicylic Acid
Reactant(s):
Methyl salicylate
Sodium hydroxide (NaOH)
Water
Product(s):
Salicylic acid (solid) ← MAIN PRODUCT
Methanol (from ester hydrolysis)
(You re-protonate salicylate with H₂SO₄ to get the solid.)
LAB 9 — Dehydration of Cyclohexanol → CyclohexeneReactant(s)
Cyclohexanol
Phosphoric acid / sulfuric acid (acid catalyst)
Product(s):
Cyclohexene ← MAIN PRODUCT (distilled off)
Water (by-product)
This is an E1 elimination.
LAB 10 — SN1 Synthesis of tert-Pentyl Chloride
Reactant(s):
tert-Pentyl alcohol (2-methyl-2-butanol)
Hydrochloric acid (HCl)
Product(s):
tert-Pentyl chloride (organic layer) ← MAIN PRODUCT
Water (by-product)
This is an SN1 reaction.