Extraction of Clove oil from Cloves by steam distillation

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5 Terms

1
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Key steps + observations in the procedure for the extraction of clove oil from cloves by steam distillation:

  • the apparatus for steam distillation is set up

  • the steam generator or copper kettle provides steam

  • the safety tube prevents a build of pressure formed by the steam

  • steam tap prevents excess steam from entering the pear shaped flask

  • liebig condenser condenses the emulsion: water in at the bottom out at the top

  • a milky emulsion is collected, a mixture of clove oil and water

2
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Draw a diagram of the steam distillation apparatus:

3
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What are safety precautions are taken during this experiment?

  • as steam is being used exercise care to avoid scalding

  • euganol can burn the skin so gloves should be worn when handling the emulsion obtained 

4
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What are some precautions taken during this experiment?

  • ensure the bottom of the safety tube is placed below the water at all times, otherwise steam would escape rather than entering the pear shaped flask

5
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Name the substance that is the main part of clove oil + draw its structure:

Eugenol (4-allyl-2-methoxy phenol)