Risk Assessments and Errors

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1
When testing for metal ions with NaOH (aq), the solution can be ^^**corrosive**^^ and extremely dangerous to eyes at a concentration of 0.5moldm^-3+.

How can you reduce this risk?
  • Use a lower concentration

  • Wear eye protection

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2
When testing for organic compounds by heating acidified potassium dichromate(VI), many of the organic molecules are ^^**flammable**^^.

How can you reduce this risk?
* Heat with a water bath instead of a Bunsen burner
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3
In the nitration of benzene, benzene is a ^^**carcinogen**^^.

How can you reduce this risk?
* Use a different aromatic compound that is a low hazard (eg methylbenzene)
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4
When testing solid halides with concentrated sulfuric acid, the concentrated sulfuric acid is ^^**very corrosive**^^.

How can you reduce this risk?
* Wear gloves
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5
When testing reaction kinetics in sodium thiosulfate + acid reaction, ^^**toxic**^^ sulfur dioxide ^^**gas**^^ is produced.

How can you reduce this risk?
  • Do the experiment in a fume cupboard

  • Do the reaction on a very small scale to minimise amount of gas produced

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6
How can you find experimental error as a percentage?
(Real answer - experimental answer/ Real answer) x100
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7
Does experimental error need to be positive or negative?
No, just put the value
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8
What does it mean if experimental error is higher than apparatus error?
Result is still accurate
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9
What makes a result inaccurate?
If experimental error is greater than apparatus error
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10
How do you find the apparatus uncertainty for a normal measurement?
(margin of error/ quantity measurement) x 100
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11
How do you find the apparatus uncertainty for a change in something? Eg temp, mass
2 x (margin of error/ quantity measured) x 100
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12
How can you find total apparatus uncertainty?
Add together the apparatus uncertainties of all equipment used
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