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260 nm
Nucleic acid absorb strongly at ____
Polymerase Chain Reaction
What does PCR stands for?
260 and 280
the ratio that gives an estimate of the purity of nucleic acid
260/280 ratio of 1.8-2.0
Pure preparations of DNA
1.8-2.0
ratio of pure preparation of DNA
260/280 ratio 1.8-2.0
260/230 ratio 2.0-2.2
DNA Template
260/280 ratio 2.0
RNA Template
1-5mM
Mg2+ concentration
Increased sensitivity, Decrease specificity
Increase Mg id equivalent to:
0.1-0.6 uM
Primer concentration
5 C - 10 C below melting temp of primers
Annealing temperature
50-500 uM
dnTP concentration
0.5-3.5 units / 50 uL
DNA polymerase
Gradient PCR
Generate a temperature gradient for the annealing step
focused on the annealing temperature
Thermus aquaticus (Taq)
Isolated from hot spring dwelling bacterium
Not destroyed at 94 C
Optimal temperature is 72 C
Error rate 3.0 × 10-4
Widely used for endpoint PCR
72 C
Optimal temperature for heat table DNA polymerase
3.0 × 10-4
Error rate for Heated Stable DNA Polymerase
Taq
Widely used for endpoint PCR
Thermus aquaticus (Taq)
Stabilizes the entire DNA polymerase process
Thermostable DNA polymerase that catalyzes the primer-dependent incorporation of nucleotides into duplex DNA in the 5’ → 3’ direction in the presence of Magnesium
Does not proof read
Error rate 1 per 3,300 bases
Newer polymerase have high fidelity
Problems with Taq
Pyrococcus furiosus (Pfu)
Hyperthermophilic archaeon
3’-to-5’ exonuclease activity
Excellent for GC-rich templates
Error rate 1 per 1,000,000 bases
Applications: cloning, DNA sequencing
Pyrococcus furiosus
What does Pfu stands for?
230
At what absorbance indicates the presence of phenol
280
At what absorbance indicates the presence of protein
Gradient PCR
Optimize the reaction in one PCR run
94 C
Taq is not destroyed at what temperature?
3’-5’
Exonuclease activity of Pfu
High Fidelity DNA Polymerase / Pfu
Excellent for GC-rich templates
1 per 1,000,000 bases
error rate of High Fidelity DNA Polymerase
Cloning
DNA Sequencing
Applications of High Fidelity DNA Polymerase / Pfu