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steps to use IR spectroscopy
clean the top plate with ethanol and allow the plate to air dry every time
inspect the underside of the press for any contamination
turn the press until the pressure indicator in the screen in about halfway green
If the pressure indicator turns red, you need to unscrew the press. The anvil can crack.
percentage transmittance.
How much of a particular frequency gets through the compound
fingerprint region.
The region to the right-hand side of the diagram (from about 1250 to 400 cm-1)
The pattern in the fingerprint region is completely different and could therefore be used to identify the compound.
functional group region
4000 cm^-1 to 1250 cm^-1
the more H-bonding, the ___ in the functional group region
the wider the peaker
the greater the absorption
what if we have peaks that aren’t supposed to be therer?
that means impurities are present
leftover starting material
IR rules
clean the area around the instrument
clean the instrument with isopropyl alcohol
don’t wear gloves
follow instructions above computers
look at IR after it printed