16- Melting point and purity

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Last updated 3:32 PM on 8/19/26
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10 Terms

1
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How can the purity of an organic solid be tested?

Determine its melting point or melting range and compare it with a quoted value.

2
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What does a very pure sample have as its melting point?

A sharp melting point at the quoted data-book value.

3
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What happens to melting point when impurities are present?

The melting point is lowered.

4
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What happens to the melting range when impurities are present?

The sample melts over a range of several degrees Celsius.

5
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What can count as an impurity after recrystallisation?

Residual solvent.

6
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Why should the sample be heated slowly near its melting point?

To obtain an accurate melting point.

7
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What can cause an error when measuring melting point?

The thermometer temperature may not be the same as the actual temperature of the sample.

8
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What equipment can be used to measure melting point?

An electronic melting point machine or a capillary tube attached to a thermometer in heating oil.

9
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What properties should the heating oil have?

A boiling point higher than the sample's melting point and low flammability.

10
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What is the key exam phrase for impurities?

“Impurities lower the melting point and cause the sample to melt over a range.”