Synthesis of carboxylic acids

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Last updated 2:43 AM on 8/10/26
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5 Terms

1
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Primary alcohol to COOH

Jones oxidation conditions

(Na2cr2o7/h2so4/h2o acetone)

or

NaOCl in water

know mechanism

2
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Cyclohexene to r-cooh

Oxidative cleavage

1) concentrated KMnO4 and heat

Then 2) acid water work up

3
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Cyclohexene with a methyl on it (it is most sub alkene so mehtyl attached to like a side of the alkene) to r-cooh

1) O3 (ozone), MeOH, CH2Cl2

Then 2) H2O2 or mcpba (meta-chloroperoxybenzoic acid) it is like some kind of of peroxyacid

4
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Internal alkyne thing to COOH

1) O3, MeOH, CH2Cl2

Then 2) H2O or acid water work up

Makes TWO cooh

5
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Grignard to cooh

r-x plus Mg0 and et2o to r-mgx

1) dry ice CO2(s)

2) acid water work up

know mechanism