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Purpose of this experiment
Synthesize banana oil via reflux, and confirm the reaction occurred using IR and GC
Ester
COOR
What are esters for
Strong Odors
Artificial flavouring
isopentyl acetate
What are you forming in this equation
isopentyl acetate
How is this ester formed?
Fischer Esterification
Process
heat carboxylic acid with alcohol with catalyst
How do you increase reaction efficiency?
Apply Le Chat’s principle to shift equilibrium towards products
How can you obtain pure component?
Separate using solubilities, boiling points, acid base properties, etc
What is the mixture at the end of reflux? (4)
Unreacted acetic acid, sulfuric acid, water, unreacted isopentyl alcohol
Water
will be separated from the ester
Isopentyl acetate
insoluble in water
Aqueous sodium bicarbonate
convert acid to salts