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Distillation

Simple

Setup

  • Flask - contains liquid solution

  • Bun - seals flask so no gasses can escape

  • Thermometer - placed through bun to measure temp inside the flask

  • Condenser - attached to a water jacket to provide a stream of continuously flowing cold water

  • Beaker - at the end of the condenser to capture pure liquid

  • Bunsen burner - placed beneath the flask to heat the solution

Process

  • Heat the mixture using a Bunsen burner so that desired liquid evaporates

  • As the gas rises to the top of the flask, the pressure will force it into the condenser

  • Because their is a continuous flow of cool water, the gas will condense back into liquid where it is collected in the beaker.

Fractional

Setup

  • Flask - contains mixture

  • Bun - seals beaker to prevent gasses escaping

  • Fractioning column - filled with tiny glass tods to maximise surface area and cooler at the top then the bottom to prevent unwanted gasses evaporating

  • Condenser - attached to water jacket to provide a continuous flow of cool water

  • beaker - collects pure liquid provided by the condenser

  • Bunsen burner - heats mixture in flask

Process

  • Flask filled with a mixture containing different liquids of different boiling points

  • Flask is heated by Bunsen burner at temperature of the liquid with the lowest boiling point

  • This liquid then travels through the fractioning column and is forced into the condenser due to the pressure

  • Due to continuous flow of cool water provided by the water jacket the gas condenses back to water and is collected in the beaker

  • If any of the other liquids somehow evaporate, the fractioning column condenses them back to liquid as the glass rods are cooler than their boiling points

  • Process is repeated at the temperature of each mixtures individual boiling points.

Distillation

Simple

Setup

  • Flask - contains liquid solution

  • Bun - seals flask so no gasses can escape

  • Thermometer - placed through bun to measure temp inside the flask

  • Condenser - attached to a water jacket to provide a stream of continuously flowing cold water

  • Beaker - at the end of the condenser to capture pure liquid

  • Bunsen burner - placed beneath the flask to heat the solution

Process

  • Heat the mixture using a Bunsen burner so that desired liquid evaporates

  • As the gas rises to the top of the flask, the pressure will force it into the condenser

  • Because their is a continuous flow of cool water, the gas will condense back into liquid where it is collected in the beaker.

Fractional

Setup

  • Flask - contains mixture

  • Bun - seals beaker to prevent gasses escaping

  • Fractioning column - filled with tiny glass tods to maximise surface area and cooler at the top then the bottom to prevent unwanted gasses evaporating

  • Condenser - attached to water jacket to provide a continuous flow of cool water

  • beaker - collects pure liquid provided by the condenser

  • Bunsen burner - heats mixture in flask

Process

  • Flask filled with a mixture containing different liquids of different boiling points

  • Flask is heated by Bunsen burner at temperature of the liquid with the lowest boiling point

  • This liquid then travels through the fractioning column and is forced into the condenser due to the pressure

  • Due to continuous flow of cool water provided by the water jacket the gas condenses back to water and is collected in the beaker

  • If any of the other liquids somehow evaporate, the fractioning column condenses them back to liquid as the glass rods are cooler than their boiling points

  • Process is repeated at the temperature of each mixtures individual boiling points.

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