Clearly state the aim of the experiment.
Explain the theory behind the experiment succinctly, limiting to no more than half a page.
Include academic references in Harvard format, ideally a minimum of three references.
Use clear and concise language to express the aim and underlying concepts.
Ensure that the introduction flows logically and transitions well between points.
The introduction should condense important information into a brief overview (around 10% of the total report).
Use Harvard referencing style for all sources cited in the introduction. Ensure to properly format both in-text citations and the reference list.
Preparation of Sodium Carbonate:
Prepare a standard solution of sodium carbonate.
Determining HCl Concentration:
Use the prepared sodium carbonate solution to find the concentration of hydrochloric acid (HCl) solution of approximately 0.1 mol dm³.
Determining RMM of a Primary Amine:
Use the HCl solution to assess the relative molecular mass (RMM) of a primary amine with the formula Ph-CH(R)-NH2 (where Ph stands for benzene ring).
Identifying Group R:
Based on the results, suggest the identity of the group R in the amine formula.
Read the entire method and COSHH (Control of Substances Hazardous to Health) form before attending the lab to ensure safety and understanding of procedures.
The primary aim of the experiment is to determine the relative molecular mass (RMM) of a primary amine using titration methods.
Focus will be on identifying the unknown alkyl ('R') group associated with the amine.
Titration involves adding an acid to a basic solution while monitoring the reaction using an indicator to determine the reaction endpoint.
The technique involves a standard solution of known concentration for accurate analysis.
Amines are organic compounds containing nitrogen and can be categorized as primary, secondary, or tertiary based on the number of hydrogens replaced by alkyl groups.
Titration is useful for calculating concentrations and has historical significance in analytical chemistry.
Johansson A. (1988). "Analytica Chimica Acta: The development of titration methods: Some historical annotations."
Crowe and Bradshaw (2021). "Essential contributions to analytical chemistry."
Lewis and Evans (2018). "Acid-Base Reactions and Titrations: A guide for practitioners."
Exceptional (90-100%): Outstanding research and clarity in presentation; exceptional understanding of experiment aim and theory.
Very Good (70-89%): High-level research; very minor errors; good clarity.
Satisfactory (40-49%): Adequate research; some clarity issues.
Unsatisfactory (35-39%): Poor research; significant misunderstandings.
Aim: Determine RMM of primary amine using titration; methodology explained clearly.
Discusses titration as a method for analyzing solutions and gaining insight into amine structures; involves historical context.
Explanation of titration in forensic science; demonstrations of reagent reactions and analysis importance.
Shows concise aim formulation; clarity on acid-base reactions and importance in broader contexts.
Provides an overview of the methodology, emphasizing procedural details for clarity and insight into results.