AldehydesKetones 9
Page 1: Introduction
Course Title: PHAR201 Towards unbounded Carbonyl Compounds
Focus on Aldehydes & Ketones
Instructor: Dr. Mohamed Salah (M.Salah@ngu.edu.eg)
Institution: School of Pharmacy, NGU
Page 2: Learning Outcomes
Describe chemical characteristics and reactivity of functional groups.
Understand stereochemistry of drugs and its relation to drug activity and toxicity.
Explain the importance of structure and bonding in drug molecules.
Discuss effects on molecular shape, physical properties, chemical properties, and interactions with other molecules.
Evaluate their pharmaceutical use.
Page 3: Overview
Introduction to carbonyl compounds
Nature of carbonyl group
Aldehydes and Ketones
A. Nomenclature
B. Reactivity
Nucleophilic Addition Reactions
Page 4: Carbonyl Compounds - Introduction
Pronunciation: car-bo-neel
Ubiquity of carbonyl compounds in nature (e.g. citric acid, acetaminophen).
Presentation as part of many functional groups.
Page 5: Types of Carbonyl Compounds
A. Aldehydes and Ketones (1 Lecture)
B. Carboxylic Acids and their Derivatives (2 Lectures)
Page 6: Nature of the Carbonyl Group
Carbon–oxygen double bond of carbonyl is analogous to carbon–carbon double bond of alkenes.
Page 7: Structure of the Carbonyl Group
sp2 hybridization of carbon and oxygen results in a planar structure.
Page 8: Polarization of the Carbonyl Group
Carbon–oxygen double bond is strongly polarized due to oxygen's high electronegativity.
Electrophilic (Lewis acidic) sites and nucleophilic (Lewis basic) sites are established.
Page 9: Hydrogen Bonding Effects
Hydrogen bonding influences boiling points and solubility of aldehydes and ketones.
Example: Pentanal (69°C boiling point) vs. Pentan-1-ol (102°C boiling point).
Page 10: Naming Aldehydes
The parent chain must contain the –CHO group (Carbon 1 is the carbonyl carbon).
Aldehydes are named by replacing the ‘-e’ in the alkane name with ‘-al’.
Page 11: Common Names of Simple Aldehydes
HCHO: Formaldehyde
CH3CHO: Acetaldehyde
CHO: Benzaldehyde
Page 12: Naming Ketones
Longest chain containing the ketone group is the parent chain.
Numbering starts from the end closest to the carbonyl carbon.
Naming involves replacing ‘-e’ in the alkane name with ‘-one’.
Page 13: Common Names of Simple Ketones
CH3C(CH3)2: Acetone
C6H5C(O)R: Acetophenone
C6H5C(O)C6H5: Benzophenone
Page 14: Alpha Proton Acidity
Definition of α Proton (adjacent to carbonyl).
Weakly acidic due to resonance stabilization of the conjugate base.
Page 15: Effect of Multiple Carbonyls
Acidity of α Protons is increased with multiple carbonyl groups.
Example: penta-2,4-dione has a pKa of 9.
Page 16: Nucleophilic Addition Reactions
Introduction to the concept of nucleophilic addition reactions involving carbonyl compounds.
Page 17: Mechanism of Nucleophilic Addition
Nucleophile adds to electrophilic carbon of C=O group.
Rehybridization of carbon from sp2 to sp3.
Movement of electron pair from C=O bond to oxygen.
Formation of tetrahedral alkoxide ion intermediate.
Protonation of the alkoxide ion.
Page 18: Aldehydes vs Ketones
Aldehydes are generally more reactive than ketones for two reasons:
Steric hindrance - fewer steric hindrances in aldehydes.
Electronic factors - Aldehydes show greater polarization in carbonyl than ketones.
Page 19: Aldehydes vs Ketones - Sterics
One large substituent in aldehydes allows easier nucleophile approach as compared to two large substituents in ketones.
Page 20: Aldehydes vs Ketones - Electronics
Greater polarization in aldehyde carbonyls compared to ketones contributes to their reactivity.
Page 21: Reaction with Alcohols
Aldehydes and ketones react with alcohols to create hemiacetals or hemiketals.
Page 22: Nucleophilic Addition-Elimination Reactions
Primary amines react with aldehydes/ketones to yield imines (Schiff bases).
Page 23: Reaction Mechanism with Amines
Addition of amine to carbonyl forms a dipolar tetrahedral intermediate.
Proton transfer from nitrogen to oxygen yields an amino alcohol intermediate.
Dehydration forms an imine and water as final products.
Page 24: Example of Amines Reaction
Example: The amino acid alanine reacts with pyridoxal phosphate to yield an imine.
Page 28: References
McMurry, J. Organic Chemistry, 9th edition, 2019.
Sarker, S. D. and Nahar, L. Chemistry for Pharmacy Students.
Page 29: Conclusion
Encouragement towards unbounded thinking.
Reminder of NGU School of Pharmacy thanks.