Enzyme Regulation Notes

Enzymes - Regulation

Controlling Enzyme Activity

  • Enzymes need control mechanisms to prevent them from being constantly active or inactive.
  • Analogous to a car needing brakes and an accelerator.
  • Enzymes respond to environmental factors by speeding up or slowing down.

Allosteric Enzymes

  • Have more than one binding site:
    • Active site: where the substrate binds.
    • Allosteric site: where a regulatory molecule binds.
  • Switch between two conformations: active and inactive.
  • Binding of a regulatory molecule (ligand) changes the activity by stabilizing one of the two conformations.

Aspartate Transcarbamoylase

  • Regulated by the binding of cytosine triphosphate (CTP).
  • CTP binding to regulatory sites switches the enzyme to an inactive form.
  • Illustrates allosteric regulation.

Kinetics of Allosteric Enzymes

  • Allosteric enzymes may not follow Michaelis-Menten kinetics.
  • They often exhibit sigmoidal curves instead of hyperbolic curves, unlike Michaelis-Menten enzymes.

Feedback Inhibition

  • Metabolic pathways often involve a series of enzymes.
  • The final product of the pathway often inhibits an enzyme at the start of the pathway.
  • This is called feedback inhibition and prevents wasteful overproduction.

Mechanism of Feedback Inhibition

  • Once enough of the final product (F) is produced, it inhibits enzyme e1.
  • e1 is typically an allosteric enzyme regulated by the binding of F.
  • The regulated enzyme (e1) catalyzes the committed step in the pathway.

Aspartate Transcarbamoylase and Feedback Inhibition

  • Regulation of aspartate transcarbamoylase is a type of feedback inhibition.
  • The enzyme catalyzes the first step in CTP synthesis.
  • The product, CTP, inhibits aspartate transcarbamoylase by binding to the inactive form.

Allosteric Regulation by ATP and CTP

  • CTP is an allosteric inhibitor of aspartate transcarbamoylase.
  • ATP is an allosteric activator of aspartate transcarbamoylase.
  • The rate of N-carbamoylaspartate formation varies with aspartate concentration, and is affected by the presence of ATP or CTP.

Allosteric Proteins and Cooperativity

  • Show cooperativity and sigmoidal kinetics with regard to their substrate.
  • Bind ligands (effectors) that are not their substrates.
  • Effectors bind at effector binding sites, separate from the ligand binding site.
  • Effector binding influences the affinity of the protein subunits for the ligand.
    • Positive effectors increase affinity.
    • Negative effectors decrease affinity.

Effect of Effectors on Sigmoidal Curve

  • Positive effectors:
    • Steeper slope of the v (velocity) against [S] (substrate concentration) graph.
    • The v against [S] graph shifts from right to left.
    • Higher v for the same [S] until saturation.
    • Smaller change in [S] for the same change in v.
  • Negative effectors: Opposite effects.

Clinical Example - Oxygen Carrying Proteins

  • Myoglobin and hemoglobin.
  • Contain protein globin and the haem grouping.
  • The Fe^{2+} in the center of the haem group binds to oxygen; iron must be in the ferrous (II) oxidation state for effective binding.

Myoglobin

  • Stores oxygen in the muscle.
  • High saturation with O2 at pO2 of interstitial fluid, so sequesters O_2 into cell.
  • Releases O2 as pO2 falls during muscular activity.

Hemoglobin

  • Transports oxygen from the lungs to the tissues.
  • Adult hemoglobin (HbA) made up of 4 subunits: 2 α subunits and 2 β subunits, each with a haem group.
  • A molecule of hemoglobin can bind four molecules of O_2.
  • Hemoglobin is an allosteric protein exhibiting cooperativity of binding for oxygen.
  • The binding curve is sigmoidal in shape.

Hemoglobin Oxygen Binding

  • High saturation with O2 at pO2 of lungs, but low saturation at pO_2 of tissues.
  • Releases O2 to tissues due to lower pO2.
  • Sigmoid curve demonstrates cooperativity.

2,3-Bisphosphoglycerate (BPG)

  • Pure HbA in a test tube binds O_2 more efficiently than HbA in the blood due to the presence of BPG in the blood.
  • BPG acts as a negative effector, resulting in more O_2 delivered to the tissues.
  • BPG concentrations in blood increase when insufficient oxygen is getting to the tissues (e.g., cardiopulmonary insufficiency, high altitude).

Hemoglobin and BPG

  • In the presence of the negative effector BPG, hemoglobin releases more O_2 to the tissues than in the absence of the effector.

Foetal Hemoglobin (HbF)

  • Made of 4 subunits: 2 α and 2 γ instead of 2 β.
  • Binds oxygen more strongly than HbA because it has a lower affinity for BPG.
  • In the placenta, both maternal and foetal tissue are at the same pO_2.
  • HbF must be able to bind O2 more tightly than HbA so that O2 is transferred from maternal blood to foetal blood.

HbF and Oxygen Transfer

  • The lower affinity for BPG by HbF reduces sigmoidicity of the curve and allows it to take up O2 from HbA at pO2 in the placenta.
  • HbF in blood + BPG has a higher % Saturation than HbA in blood + BPG at the pO_2 of tissues, allowing O2 transfer.

HbF Efficiency

  • HbF is very efficient for the uptake of O_2 across the placenta.
  • HbF is not as efficient as HbA in transferring O_2 from lungs to tissues.
  • A few weeks before birth, γ chains cease to be produced and are replaced by β chains.
  • Until all HbF in neonatal blood is replaced by HbA, the infant has lower efficiency than an adult at transferring O_2 from lungs to tissues.
  • To counteract this, neonates/infants have a higher total Hb concentration in blood.

Models of Allosteric Action

  • Two models describe allosteric effects:
    • Concerted model.
    • Sequential model.
  • Probably a mixture of both in most enzymes.

Concerted Model (Monod, Wyman, Changeux)

  • Subunits can exist in only two forms: T (low affinity) and R (high affinity).
  • Cannot have mixed molecules (i.e., subunits are either all T or all R).

Cooperativity in Concerted Model

  • When the substrate binds to the T form, it causes all subunits to convert to the R form.
  • Because the R form has a higher affinity for the substrate than the T form, enzyme activity increases rapidly after each enzyme molecule has bound one substrate molecule.

Sequential Model (Koshland)

  • Subunits can exist in two forms: T (low affinity) and R (high affinity).
  • Can have mixed molecules (i.e., some subunits can be T while others are R).

Cooperativity in Sequential Model

  • When the substrate binds to the T form, it causes the subunit to which it binds to convert to the R form and makes it easier for the substrate to bind to the other subunits.
  • Because the affinity for the substrate increases once one subunit has converted to the R form, activity increases rapidly after the protein has bound one substrate molecule.

Summary of the Models

  • In both models:
    • Positive effectors stabilize the high affinity form of the subunits.
    • Negative effectors stabilize the low affinity form of the subunits.

Enzyme Kinetics and Inhibitors Summary

  • Some enzymes are allosterically regulated by inhibitors or activators.
  • Enzyme inhibitors can be reversible or irreversible.
  • Competitive reversible inhibitors increase apparent KM, but do not affect V{max}.
  • Noncompetitive inhibitors decrease apparent V{max}, but do not affect KM.
  • Irreversible inhibitors usually bind covalently to enzymes.
  • Many important drugs are enzyme inhibitors.