d and f block elements

Unit- 8 The d & f Block Elements

  • Presented by: Rajesh Kumar G, PGT Chemistry, JNV Kollam, Kerala, Hyderabad Region

d-Block Elements

Introduction

  • Definition: Elements belonging to groups 3 to 12 of the periodic table.

  • Electron Configuration: Last electron enters into the penultimate d-orbital.

  • Position: d-block elements lie between s-block and p-block elements.

Outline

  • Key Topics:

    • Transition Series

    • General Electronic Configuration

    • General Characteristics:

      • Melting and Boiling Point

      • Atomic and Ionic Size

      • Ionisation Enthalpy

      • Oxidation State

      • Reactivity

      • Magnetic Properties

      • Standard Electrode Potential

Periodic Table Overview

  • Notable Groups:

    • IA: Alkali Metals

    • IIA: Alkaline Earths

    • VIIA: Halogens

    • Noble Gases: Group 18

  • Transition Metals: Scandium to Zinc and their properties.

Transition Series

  • Four Transition Series:

    • 1st Transition Series (3d series): Sc to Zn

    • 2nd Transition Series (4d series): Y to Cd

    • 3rd Transition Series (5d series): La, Hf to Hg

    • 4th Transition Series (6d series): Ac, Rf to Cn

Transition Elements

  • Definition: Elements with partially filled penultimate d-subshell in their ground state or most common oxidation state.

  • Notable Exceptions: Zn, Cd, and Hg are not considered transition elements.

General Electronic Configuration

  • Electronic Configuration: (n-1)d^10 ns¹-²

  • Example (3d Series):

    • Sc: [Ar] 3d¹ 4s²

    • Ti: [Ar] 3d² 4s²

Properties of Transition Elements

General Properties

  • Magnetic Properties: Due to unpaired electrons.

  • Color: Formation of colored ions.

  • Complex Formation: Ability to form coordination complexes.

  • Catalytic Properties: Due to variable oxidation states and d-orbitals.

  • Size: Trends in atomic and ionic size.

  • Melting and Boiling Points: D-block elements typically have high melting and boiling points due to strong metallic bonds.

Melting and Boiling Points

  • General Trends:

    • High melting and boiling points due to unpaired electrons.

    • Exception: Zn, Cd, and Hg have low melting points.

    • Group 6 (Cr, Mo, W) show the highest melting points.

Atomic and Ionic Radii

  • Decrease in atomic size from left to right in the periodic table.

  • Notable increase at the end of the series, particularly in 4d and 5d series due to lanthanoid contraction.

Ionisation Enthalpy

  • Generally increases from left to right.

  • Weak shielding by 4f electrons in 5d series leads to high ionization enthalpy.

Oxidation States

  • Vary widely due to small energy differences between (n-1)d and ns subshells.

  • Maximum oxidation state can reach +7 (shown by Mn).

Reactivity of Transition Elements

  • Moderately electropositive, not highly reactive due to high heat of sublimation and high ionization enthalpy.

Magnetic Moment

  • Types:

    • Paramagnetic: Due to unpaired electrons.

    • Diamagnetic: No unpaired electrons, repel from magnetic fields.

  • Magnetic moment calculated using the formula: µ = √[n(n+2)] BM, where n = number of unpaired electrons.

General Properties of d-Block Elements

  • Formation of complex compounds.

  • Exhibit catalytic properties.

  • Form colored compounds due to d-d transitions.

Potassium Dichromate (K2Cr2O7)

Preparation

  • Process from Chromite ore (FeCr2O4).

Properties

  • Orange-red crystalline compound, moderately soluble in cold water.

Uses

  • Primary standard in volumetric analysis, tanning of leather, and photographic processing.

Potassium Permanganate (KMnO4)

Preparation

  • Derived from pyrolusite ore (MnO2).

Properties

  • Purple crystalline compound, shows strong oxidizing properties in various media.

Uses

  • Laboratory oxidizing agent, antiseptic, and reagent in qualitative analysis.

Inner Transition Elements (f-block)

Definition

  • Include lanthanides and actinides.

  • Last electron enters pre-penultimate f-subshell.

Physical and Chemical Properties of Lanthanides

  • Dense metals with high melting points.

  • Sensitive to oxidation and form basic oxides.

Chemical and Industrial Applications of Actinoids

  • Used as nuclear reactor fuels (U and Pu), radioactive properties.

Differences Between Lanthanides and Actinoids

  • Radioactivity: Actinoids are generally more radioactive.

Use of Inner Transition Elements

  • Widely used in various industrial and chemical applications.