Lecture 28 notes Chapter 21 proton motive force_BCH400 spring 2025 v1 copy

Page 1: Introduction to Peter Mitchell and Chemiosmotic Theory

Peter Mitchell

  • Life: 1920-1992

  • Nobel Prize: 1978 for the Chemiosmotic Theory

  • Significant Concept: A proton concentration gradient serves as an energy reservoir for ATP formation.

Key Concept

  • Proton Motive Force (PMF): The driving force for ATP synthesis.


Page 2: Understanding Proton-Motive Force (PMF)

Definition of PMF

  • PMF is used to drive ATP synthesis by creating an electrochemical gradient.

  • It is a combination of:

    1. Chemical Gradient (DpH): Represents the pH difference across the membrane (0.5 – 0.75) contributing 85% to energy.

    2. Electrical Potential (DY): Ranges from ~140 to 170 mV.

Chemiosmotic Hypothesis

  • ATP synthesis is powered by the movement of protons across the membrane, based on the chemiosmotic hypothesis.


Page 3: Contributors to PMF

Key Contributors to Proton-Motive Force

  • Greatest Contributor: Charge gradient generated by protons.

  • Other Contributors:

    • Flux of pyruvate into the matrix

    • Rate of ATP synthesis

    • Concentration gradient of protons

    • Current from electron flow within the inner mitochondrial membrane


Page 4: Explanation of PMF Contribution

Determining Contributors

  • Charge and Concentration Gradients: Both contribute to the free energy associated with PMF.

    • DG = -2.303 RT DpH

    • Charge gradient contributes approximately 85% of the free energy.

  • Free Energy Calculations:

    • ∆G for 1 proton through FoF1 = -19.4 kJ/mol.

    • ∆G for ATP synthesis from ADP + P = +32 kJ/mol.

ATP Synthesis Calls for Multiple Protons

  • Must move more than one proton for ATP synthesis


Page 5: Evidence for Chemiosmotic Hypothesis

Experiments and Findings

  • Chemiosmotic Hypothesis Evidence:

    • ADP + Pi -> ATP requiring proton flow.


Page 6: Experimental Confirmation of PMF

Experiment Details

  • Artificial Vesicles: Created with bacteriorhodopsin and ATP synthase.

  • Bacteriorhodopsin: A light-activated proton pump. Jan

  • Findings: The ATP synthesis occurred due to proton pumping into the vesicle when illuminated, verifying the separation of the respiratory chain and ATP synthase, linked by proton-motive force.


Page 7: Mitochondrial Functioning Without Light

PMF in Dark Conditions

  • Mitochondria can operate and produce PMF independent of light; it comes from the Electron Transport Chain.

  • Summary of Components Involved:

    • ADP + Pi -> ATP

    • H+

    • Matrix & Intermembrane space roles in ATP production.


Page 8: Structure of ATP Synthase

Composition of ATP Synthase

  • F0 Component: Embedded in the inner mitochondrial membrane containing the proton channel (with 8 to 15 c subunits).

  • F1 Component: Contains active sites for ATP synthesis (three active sites on β subunits).

  • Components Connection: γ stalk connects F1 and F0, facilitating ATP production.


Page 9: Binding Change Mechanism of ATP Synthesis

Conformations of β Subunits

  • The three forms:

    • O (Open): Nucleotides can bind/releases.

    • L (Loose): Traps nucleotides.

    • T (Tight): Synthesizes ATP from ADP + Pi.

γ Subunit Role

  • Rotation of γ subunit interconverts the β subunits during ATP synthesis.


Page 10: ATP Release Mechanism

Mechanism of ATP Release

  • T-form converts ADP + Pi into ATP but doesn’t release it.

  • Rotation of γ subunit (120° CCW) converts T-form to O-form, allowing ATP release and binding of new ADP + Pi.


Page 11: Distinction between ATP Formation Mechanisms

Mechanisms Overview

  • Binding Change Mechanism: Indicates mechanical changes during ATP formation different from substrate-level phosphorylation (direct transfer of high-energy phosphate to ADP).


Page 12: Visualization of γ Subunit Rotation

Experimental Setup

  • Cloned α3β3γ subunits visualization of γ rotation during ATP hydrolysis.

  • Movement: Attachment of actin filament to γ subunit shows rotation as power is derived from ATP hydrolysis.


Page 13: Proton Flow Through ATP Synthase

c Ring Proton Movement

  • Protons move through the F0 component of ATP synthase, causing rotation:

    • Protons enter intermembrane space half-channel, bind to c ring glutamate/aspartate.

    • Rotation allows release into the matrix half-channel.


Page 14: Proton Flux and c Ring Operation

Mechanism Overview

  • Mechanism of Rotation: The neutralization of negative charge allows c ring subunits to rotate and produce ATP.


Page 15: Efficiency of Vertebrate ATP Synthase

ATP Production Efficiency

  • Vertebrate c ring: Composed of 8 subunits.

  • Proton Requirement: One full rotation requires 8 protons, producing 3 ATP molecules.

  • Significance: The number of c ring subunits directly affects ATP synthesis efficiency.


Page 16: Entry of NADH Electrons

Mechanisms for NADH Entry

  • NADH Transport: Requires mechanisms (shuttles) to transfer electrons from cytoplasm into mitochondria.

  • ATP Transport: Mechanisms also exist for newly synthesized ATP to exit.


Page 17: Glycerol 3-Phosphate Shuttle

Shuttle Functionality

  • Transfers electrons from NADH to FAD to QH2.

  • Important in specific metabolic contexts like insect flight muscles.


Page 18: Malate-Aspartate Shuttle

Functionality and Characteristics

  • Malate can cross the mitochondrial membrane, while oxaloacetate cannot.

  • Transfers electrons from NADH to another NADH in the mitochondrial matrix.


Page 19: ATP-ADP Translocase Mechanism

Role in Metabolite Exchange

  • ATP-ADP translocase: Exchanging one ATP out for one ADP in.

  • Various carriers for other metabolites require energy (~25% of oxidative phosphorylation energy).


Page 20: ATP Yield from Glucose Oxidation

ATP Production Overview

  • Out of ~30-32 ATP from glucose combustion:

    • 26-28 via oxidative phosphorylation.

    • 4 from substrate-level phosphorylation.

  • Fermentation yields only 2 ATP.


Page 21: Accounting for ATP Yield

ATP Formation Breakdown

  • Overview of contributions:

    • Substrate-level phosphorylation yields net 2 ATP.

    • NADH electrons originate from glycolysis in the cytoplasm.


Page 22: Major ATP Consumers in Eukaryotic Cells

ATP Consumption Categories

  • Processes consuming ATP:

    • 30% for protein synthesis

    • 25-35% for P-type ATPase ion pumps (Na/K and Ca ATPases).

  • Energy requirement to maintain body temperature is significant; ~20% of electron transport energy is uncoupled from ATP synthesis.


Page 23: Pyruvate and Electron Transport Shutdown

Experiment Insights

  • Mitochondrial experiments reveal that the ATP synthase ceases functioning when ADP is depleted.

  • O2 Consumption as Measure: Indicates electron flow is absent when proton gradient maxes out without ADP.


Page 24: Uncouplers and Electron Transport

Uncoupling Mechanisms

  • Uncouplers allow electron transport without ATP production by moving H+ across the membrane.

  • Historical Context: DNP was banned as a weight-loss drug due to its effects.


Page 25: Effects of 2,4-Dinitrophenol as an Uncoupler

Mechanism Overview

  • Uncouples oxygen consumption from ATP formation, keeping electron transport active by reducing proton gradient.


Page 26: Mammalian Uncoupling Mechanisms

Importance of Uncoupling Protein (UCP)

  • Mammals (excluding pigs) can uncouple electron transport to regulate body temperature.

  • Essential for newborns and hibernating animals.


Page 27: ATP Synthesis Inhibitors

Electron Transport Inhibitors

  • Key Inhibitors:

    • Rotenone

    • Cyanide

    • Azide

    • MPTP affects complex IV.


Page 28: Role of Complex IV

Functionality of Cytochrome c Oxidase

  • Complex IV catalyzes the reduction of molecular oxygen to water.

  • Toxicity of CO due to higher affinity for binding than O2.


Page 29: Understanding Rotenone

Characteristics

  • Plant-derived rotenonoid (from South America, etc.) that blocks Complex I.

  • Less effective in mammals due to absorption issues.


Page 30: Parkinson's Disease and MPTP

Connection to Parkinson's Disease

  • MPTP is a neurotoxin blocking Complex I, linked to synthetic heroin contamination.

  • Discovered link highlighted by Dr. Langston regarding its effect.

    • MPTP preferentially destroys dopaminergic neurons, crucial in Parkinson's pathology.


Page 31: Importance of Complex 1

Nutrient Metabolism Dependency

  • Complex I is essential as FADH2 cannot simply substitute without TCA cycle function.

  • TCA cycle needs NAD+ regeneration done by Complex I to function properly.