CH 11(2/6)(PG 19-20)

Critical Temperature and Pressure for CO2 Supercritical Fluids

  • Definition:
    • Critical temperature: The temperature above which a substance cannot exist as a liquid, regardless of pressure.
    • Critical pressure: The minimum pressure required to maintain a substance in its liquid state at its critical temperature.
  • Properties of Supercritical CO2:
    • Acts as an attractive solvent.
    • Capable of dissolving materials that are normally insoluble in other solvents.
    • Commonly used to extract substances such as:
    • Caffeine from coffee.
    • Food flavorings, maintaining the integrity of flavor while removing caffeine.
  • Example:
    • In the extraction process, supercritical CO2 efficiently dissolves caffeine while preserving the flavors characterizing coffee.

Surface Tension

  • Definition:
    • Surface tension is the energy required to increase the surface area of a liquid substance.
    • Less formally, it can be described as the energy needed to "break" the surface of the liquid.
  • Molecular Behavior:
    • Molecules located at the surface behave differently compared to those situated in the liquid's interior.
    • Surface molecules experience a net inward force of attraction due to the lack of neighboring liquid molecules above them, resulting in an energized surface layer.

Capillary Action

  • Definition:
    • Capillary action is defined as the movement of liquid within a narrow space, such as a capillary tube, against the force of gravity.
  • Key Factors:
    • Intermolecular forces contribute to the capillary action phenomenon.
    • The movement results in the formation of a concave meniscus in water columns.
  • Cohesive and Adhesive Forces:
    • Cohesive Forces:
    • Intermolecular forces that bind similar molecules to each other.
    • Adhesive Forces:
    • Intermolecular forces that bind a substance to a surface.
  • Meniscus Behavior:
    • When cohesive forces dominate adhesive forces, a convex meniscus forms.
    • Conversely, when adhesive forces are stronger than cohesive forces, a concave meniscus occurs.
    • Example: When water rises in a paper, it is due to the adhesive forces between water molecules (H-bonds) and the hydroxyl (OH) groups of cellulose in the paper.

Viscosity

  • Definition:
    • Viscosity is defined as the resistance of a liquid to flow.
  • Relation to Molecular Movement:
    • Viscosity is related to how easily individual liquid molecules move relative to one another.
  • Temperature Dependence:
    • Viscosity generally decreases with increasing temperature, as higher temperatures facilitate molecular movement.
  • Measurement Method:
    • Viscosity can be quantified by observing the rate at which a solid object descends through the liquid:
    • A lower rate or longer time for an object to fall indicates higher viscosity.