Coagulation Testing Study Notes

COAGULATION TESTING

SPECIMENS FOR COAGULATION TESTING

  • Purpose: Assesses in vitro coagulation.

  • Lab Testing: Measures the time required to form a clot.

  • Pre-analytical Variation: Coagulation assays are highly sensitive to variations before testing; thus, collection must be meticulously performed.

  • Collection Protocol:

    • Avoid: Tissue thromboplastin contamination, inappropriate anticoagulant contact, usage of incorrect anticoagulant, improper temperature conditions, and hemolysis to prevent adverse outcomes for the patient.

ANTICOAGULANTS

  • Blood Type: Coagulation testing is conducted on plasma.

  • Anticoagulant: 3.2% sodium citrate is used.

    • Mechanism: Citrate binds to calcium ions, inhibiting multiple steps in hemostasis, thereby preventing the blood from clotting.

  • Collection Guidelines:

    • Avoid Glass Tubes: They may activate factors XI & XII during blood draw.

    • Blood to Anticoagulant Ratio: 9 parts blood to 1 part sodium citrate.

    • Vacuum Collection: Tubes must be collected via vacuum to the designated fill line.

    • Using Expired Vacutainers: This is prohibited.

    • Clotted Specimens: Such specimens are unacceptable for assays.

COLLECTION & STORAGE

  • Importance of Preventing Carryover: Essential to avoid contamination from tubes containing other anticoagulants.

  • Collection Order: Coagulation tubes should be collected first or only after tubes without additives.

  • Venipuncture Technique: Clean and rapid to avoid contamination with tissue thromboplastin.

  • Avoid Hemolysis: This can activate coagulation factors.

  • Temperature Regulations:

    • PT specimens may be stored at room temperature for up to 24 hours.

    • APTT specimens can only remain at room temp for up to 4 hours.

  • Butterfly System Usage: If this system is utilized, a discard tube must be used to prevent air from entering the vacutainer.

SPECIMEN PROCESSING

  • Transportation: To the lab must be quick and careful.

  • Centrifugation:

    • Samples should be centrifuged to obtain platelet-poor plasma (with PLT count < 10 x 10^9/L).

    • APTT specimens need centrifugation within 1 hour post-collection; PT specimens can stay uncentrifuged up to 24 hours.

  • Testing Protocol: If testing is done immediately, plasma can be retained on packed red cells. Otherwise, plasma must be separated from cellular components.

  • Tubes: They should stay stoppered until testing; unsuitable specimens for testing include lipemic, icteric, hemolyzed, or clotted specimens.

ERRORS AFFECTING TESTING

  • Common Errors:

    • Blood drawn into an incorrect tube type.

    • Incorrect plasma to citrate ratio caused by underfilling or a hematocrit exceeding 0.550.

    • Heparin contamination from IV contamination or incorrect order of draw.

    • Clotting in the tube attributable to traumatic venipuncture or improper mixing.

PERFORMANCE OF COAGULATION ASSAYS

  • Laboratory Protocol:

    • Adhere closely to each instrument's manufacturer instructions.

    • Normal and abnormal quality controls must be executed when testing commences each day, at the beginning of new shifts, or with every test run.

    • Controls are reconstituted daily from lyophilized or frozen specimens; once prepared, controls cannot be refrozen.

    • Quality controls (QC) should always be conducted under the same conditions as patient samples.

  • Laboratory Variability: Reference ranges are specific to each lab and should be reassessed with new reagent lots, instruments, or changes in collection methods.

CLOT ASSAYS

  • Factors Addressed: Prothrombin time (PT) and activated partial thromboplastin time (APTT) form the basis for screening tests for the coagulation system's functionality.

  • Follow-up Testing: If screening tests yield abnormal results, specific factor assays are performed.

PROTHROMBIN TIME (PT)

  • Overview:

    • Primarily screens the function of extrinsic and common pathways of coagulation, addressing factors VII, X, V, thrombin, and fibrinogen.

    • Commonly used for pre-operative screenings and monitoring of Warfarin (Coumadin) and other vitamin K antagnostic therapies.

    • Testing Method: Calcium and an excess of thromboplastin are added to patient plasma; the timing for clot formation is measured.

PRINCIPLE OF PT TEST

  • Reagents Required:

    • Prothrombin reagent, a commercial preparation of tissue thromboplastin.

    • Process: Combine prothrombin reagent with patient plasma.

    • Activation: Triggers the extrinsic pathway where prothrombin converts to thrombin and fibrinogen to fibrin clot.

    • The timing from thromboplastin addition to the formation of the fibrin clot is recorded.

    • Detection: Clot formation can be inferred from increasing sample viscosity and turbidity, with endpoint determination via mechanical or optical methods.

EXTRINSIC PATHWAY

  • Involved Factors:

    • III (Tissue thromboplastin)

    • VII activated:

    • Ca++

    • Xa

    • X

    • Ca++, PF3

    • V

    • Va

    • Prothrombin (II)

    • Fibrinogen (I)

    • XIII

    • Thrombin

    • XIIIa

    • Fibrin Formation:

      • Monomer forms stable fibrin (polymer).

REPORTING & REFERENCE INTERVALS

  • Normal PT Range: 10 – 13 seconds.

  • Therapeutic Range: Greater than 25 seconds.

    • Reported as the International Normalized Ratio (INR).

  • Factors Influencing INR:

    • Patient age, body mass, liver function, nutritional status, and genetics.

  • INR Calculation: Standardizes PT reporting across different labs with varying patient demographics; each reagent batch has an assigned International Sensitivity Index (ISI).

  • INR Reference Range: 0.9 – 1.13.

    • Increasing INR correlates to increased anticoagulation and is elevated in the presence of extrinsic factor deficiencies due to liver disease or when using oral anticoagulants.

  • INR Calculation Example:

    • Given: Patient prothrombin time is 23 seconds, mean normal protime of facility 10.5 seconds, ISI = 1.2.

    • Calculation:

    • INR=racPatient<br>esultMean<br>ormalimesISIINR = rac{Patient<br>esult}{Mean<br>ormal} imes ISI

    • INR=rac23extsec10.5extsecimes1.2INR = rac{23 ext{ sec}}{10.5 ext{ sec}} imes 1.2

    • INR=(2.1905)imes1.2=2.6286INR = (2.1905) imes 1.2 = 2.6286

    • Rounded: INRextisapproximately2.53INR ext{ is approximately } 2.53.

CONDITIONS AFFECTING PT

  • Normal Results:

    • Factor VIII: Normal

    • Factor XI: Normal

    • Factor XII: Normal

  • Prolonged Results:

    • Thrombin (II): Prolonged

    • Factors V, VII, X: Prolonged

    • Warfarin and Heparin therapy: Prolonged

    • Liver disease: Prolonged

    • Vitamin K deficiency: Prolonged

    • Underfilled tube: Prolonged

ACTIVATED PARTIAL THROMBOPLASTIN TIME (APTT)

  • Screening Function: Evaluates factor deficiencies within intrinsic and common pathways, primarily for factors VIII, IX, XI, and XII.

  • Clinical Use: Commonly employed in pre-operative screenings and for monitoring heparin therapy.

TEST THEORY FOR APTT

  • Reagent Composition: Calcium chloride and partial thromboplastin (phospholipid component).

  • Process:

    • Add partial thromboplastin reagent to warmed patient plasma and activate the intrinsic pathway by adding CaCl2 to form the fibrin clot.

    • Calcium in blood binds to sodium citrate during specimen collection, losing calcium upon centrifugation, necessitating addition of these reagents for clotting.

INTRINSIC PATHWAY

  • Mechanism Overview:

    • Surface contact activates Factor XII with subsequent cascade involvement of Factors XI, IX, and VIII leading to thrombin production via the common pathway.

REPORTING & REFERENCE INTERVALS FOR APTT

  • Normal APTT Range: 25 – 40 seconds, with <35 seconds being desirable for surgical candidates.

  • Quality Control (QC):

    • Must be executed every 8 hours, abnormalities may surface from reagent deterioration, temperature variances, or instrument issues.

CONDITIONS AFFECTING APTT

  • Normal Results: Factors VII, XIII.

  • Prolonged Results: Factors I, II, V, VIII, IX, X, XI, XII with instances of both heparin and liver disease.

  • Underfilled Tube: Can also prolong APTT.

MIXING STUDIES

  • Purpose: Used for patients showing abnormally high PT or APTT.

  • Process:

    • An equal volume of patient plasma is combined with normal pooled plasma (1:1 mix) and re-tested for PT or APTT.

  • Interpretation:

    • If result normalizes, indicates factor deficiency or dysfunction. If unchanged, the specimen may contain inhibitors (e.g., heparin, oral anticoagulants, autoantibodies).

D-DIMER ASSAY

  • Definition: A degradation product of fibrin released during fibrinolysis by plasmin.

  • Usage: Primarily to rule out disseminated intravascular coagulation (DIC).

  • Reference Range: <500 ng/mL.

DIMER TESTING TECHNIQUES

  • Immunoturbidimetry (ELISA): Highly sensitive; capable of ruling out deep vein thrombosis and pulmonary embolism.

  • Particle Agglutination: Used for DIC detection; however, less sensitive, detecting dimers only at levels of 500 ng/mL.

ELEVATED DIMERS

  • Potential causes include:

    • Surgery, Trauma, Infection, Pregnancy, Cancer, Liver disease, Increasing age, Hospitalization.

    • The test shows sensitivity but lacks specificity.

THROMBIN TIME

  • Function: Assesses fibrinogen deficiencies or dysfunction and detects thrombin inhibitors, often elevated with heparin therapy.

  • Process: Patient plasma is mixed with thrombin and the time taken for clot formation is recorded.

FIBRINOGEN

  • Assessment: Activity levels of fibrinogen, with low levels indicating excessive loss (bleeding), consumption (DIC), or decreased production (severe liver disease).

  • Measurement Technique: Clauss method involves adding plasma to high thrombin concentrations, measuring clotting time, which is inversely proportional to fibrinogen activity (longer clot time = lower fibrinogen level).

ACTIVATED CLOTTING TIME (ACT)

  • Purpose: Non-automated test utilizing whole blood mixed with a clot activator.

  • Usage: Common in point-of-care testing and to monitor high-dose heparin therapy during surgical procedures.

  • Reference Range: 70 – 180 seconds.

COAGULATION TESTING METHODS

  • Methods Used:

    • Visual, Mechanical, Magnetic, Optical.

TESTING METHODS

  • Manual/Visual Method: Adding plasma and reagents to a glass tube and tilting to detect clot formation.

  • Mechanical Method: Employing warmed reagents, where a moving magnetic ball indicates clot formation.

  • Optical Method: Using photometric methods which isolate movement detection during clot formation.

AUTOMATION IN TESTING

  • Advantages: Capable of conducting large volume tests simultaneously with various assays.

  • Technology Used: Employs photometry or nephelometry to measure light scatter during clot formation.

  • Endpoints: Automated systems read optical density changes that indicate clot integrity, ensuring reagents and plasma are maintained at optimal temperatures.

CHROMOGENIC METHODS

  • Use: Synthetic chromogenic substrates are utilized to assess the activity of coagulation inhibitors on Factor X.