Lecture 5- Impression Material

Impression Materials

Importance of Impression Materials

  • The correct usage of impression materials is crucial for creating accurate dental models.

Mixing Ratios and Techniques

  • Scoop to Water Ratio: 1 line in the cup = 1 scoop of powder; most mixtures require a 1:1 ratio.

  • Three Scoops: If using three scoops of powder, fill the cup to the indicated line with water.

  • Technique: Water should be dispensed first to avoid powder clumping.

  • Mixing Process: Mix in a bowl using spatula; use a figure-eight motion for efficiency.

Composition of Alginate Impression Material

  • Key Ingredient: Soluble alginate (potassium alginate) is essential.

  • Reactor: Calcium ions are necessary for cross-linking the alginate.

  • Filler Particles: Added to increase strength and stiffness of the alginate.

Gypsum Hardener
  • This ingredient acts as an accelerator for gypsum (stone) setting, creating hard, dense casts when mixed with impressions.

  • It's not primarily for alginate but improves the cast's properties.

Retarder
  • Sodium Phosphate: Controls and lengthens setting time to allow for adequate working time.

Setting Reaction of Alginate

  • Mixing alginate powder with water creates a reaction:
    ext{soluble alginate} + ext{calcium sulfate}
    ightarrow ext{calcium alginate (gel)}

  • The gelation process is rapid; sodium phosphate as a retarder allows for more effective working time.

Working Time vs. Setting Time

  • Working Time: Time available for mixing before setting begins in the oral cavity.

  • Setting Time: The time during which the material solidifies in the mouth.

  • Typical working time varies based on the alginate type:

    • Regular set: 3-4.5 minutes

    • Fast set: 1.5-3 minutes

Influence of Temperature on Setting Time

  • Water Temperature: Cold water extends working time; hot water speeds up setting.

  • Each 10°C increase in temperature shortens setting time.

Powder to Liquid Ratio

  • Appropriate mixing ensures consistency: 16 grams of powder to 38 ml of water.

  • Always follow manufacturer’s recommendations for ratios to maintain quality.

Syneresis and Inhibition Deformation

  • Syneresis: Loss of water from the impression material causes deformation.

  • Inhibition: Absorption of water leads to a swollen impression, compromising accuracy.

  • Deformations result in inaccuracies in the cast; retaking the impression is necessary if deformation occurs.

Casting from Impression

  • After creating an impression, the gypsum is poured to create a positive cast.

  • Avoid long contact of impression with cast after gypsum sets to mitigate inaccuracies due to water absorption from the impression.

Handling Blood and Saliva in Impressions

  • Rinse and disinfect the impression before pouring the gypsum to avoid interference.

  • Ensure the impression surface is dry to prevent microbubbles from forming in the cast.

Elastomeric Impression Materials

Types of Elastomers

  1. Polysulfide: Two-paste system with good tear resistance, but has a characteristic smell due to sulfur.

  2. Polyether: Hydrophilic, sets chemically without requiring cooling, maintains accuracy for a longer period (7-10 days).

  3. Condensation Silicone: Releases ethyl alcohol as a byproduct, effect on dimensional stability, low odor.

  4. Addition Silicone: No byproduct release, best for prosthodontic procedures due to high accuracy and detail capture.

Polysulfide Composition

  • Comprises a base, catalyst, fillers, and plasticizer. Setting influenced by temperature and humidity.

  • Advantages: Good working and setting time, accurate reproduction.

  • Disadvantages: Strong sulfur smell, byproduct of water may cause shrinkage.

Polyether Composition

  • Known for dimensional stability; contains base and catalyst. Hydrophilic properties help in capturing details during impression making.

  • Advantages: Durable, precise, reduces distortion compared to other materials.

  • Disadvantages: Rigid; can be costly.

Condensation Silicone Composition

  • Characterized by a base of poly-dimethylsiloxane, common catalyst is stannous octoate.

  • Advantages: Less expensive compared to other elastomers, captures detail well, pleasant odor.

  • Disadvantages: Byproduct ethyl alcohol can cause inaccuracies; must pour within an hour.

Addition Silicone Composition

  • Base consists of polyvinyl siloxane. It's one of the most accurate types and widely used in modern dentistry.

  • Advantages: Excellent accuracy, no byproduct release, good for retakes.

  • Disadvantages: Cost is higher than other materials; potential for hydrogen gas release affecting quality if not handled properly.

Inelastic Impression Materials

Types of Inelastic Materials
  1. Plaster: Basic impression material for initial records.

  2. Impression Compound: Comes in sheets or sticks for higher temperature use.

  3. Zinc Oxide Eugenol Paste: Utilized primarily for final impressions and bite registrations; excellent detail with a strong smell due to eugenol.

Working with Inelastic Materials
  • Trails and Use: Custom trays made from impression compounds for making precise dentures; border molding ensures better fit.

  • Dimensional Stability: Adequate for clinical procedures, rigid after setting.

Summary of Properties

  • Hydrocolloids: Include agar (reversible) and alginate (irreversible).

  • Elastomers: Polysulfide, polyether, condensation silicone, and addition silicone; varied properties based on composition and usage.

  • Inelastic Materials: Less common, used primarily for specific applications in dentistry, including bite registration and denture fabrication.